1,4-Dibromobutane CAS 110-52-1 Purity >99.0% (GC) Factory

Short Description:

Chemical Name: 1,4-Dibromobutane

CAS: 110-52-1

Purity: >99.0% (GC) 

Colorless or Light Yellow Transparent Liquid

High Quality, Commercial Production

Contact: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


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Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer and supplier of 1,4-Dibromobutane (CAS: 110-52-1) with high quality. We can provide COA, worldwide delivery, small and bulk quantities available. If you are interested in 1,4-Dibromobutane, please send CAS number, quantity to us. Please contact: alvin@ruifuchem.com

Chemical Properties:

Chemical Name 1,4-Dibromobutane  
Synonyms 1,4-Dibromo Butane; Tetramethylene Bromide; 1,4-Butylenedibromide; 1,4-Dibrombutan; Tetramethylene Dibromide; α,ω-Dibromobutane 
Stock Status In Stock, Production Capacity 50 Tons per Month  
CAS Number 110-52-1
Molecular Formula C4H8Br2
Molecular Weight 215.92  
Melting Point -20℃(lit.)
Boiling Point 194.0~196.0℃ at 760mmHg
Flash Point 131℃(267°F)
Density 1.808 g/mL at 25℃(lit.) 
Refractive Index n20/D 1.519(lit.) 
Sensitive Air Sensitive, Light Sensitive
Water Solubility  Immiscible With Water
Solubility  Soluble in Acetone, Ether, Chloroform, Ethanol
Shipping Condition  Ambient Temperatures
COA & MSDS Available
Sample  Available
Brand Ruifu Chemical

Specifications:

Item Specifications
Appearance Colorless or Light Yellow Transparent Liquid (Eye-Measurement)
Purity / Analysis Method >99.0% (GC) 
Moisture (by K.F) ≤0.05%
PH Value 6.0~8.0 (1:1 Water Solution)
Refractive Index n20/D 1.517~1.521
Total Impurities <1.00%
Infrared Spectrum Conforms to Structure
Test Standard Enterprise Standard
Main Usage
Organic Synthesis Intermediates 

Package & Storage:

Package: Fluorinated Bottle, 25kg/Drum, 180kg/Drum, or according to customer's requirement.

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Storage Condition: Store in sealed containers at cool, dry and ventilated warehouse away from incompatible substances. Protect from air, light and moisture. 

Stability: Stable. Combustible.Incompatible With Strong Oxidizing Agents, Strong Bases.

Advantages:

Sufficient Capacity: Sufficient facilities and technicians

Professional Service: One stop purchasing service

OEM Package: Custom package and label available

Fast Delivery: If within stock, three days delivery guaranteed

Stable Supply: Maintain reasonable stock    

Technical Support: Technology solution available

Custom Synthesis Service: Ranged from grams to kilos

High Quality: Established a complete quality assurance system

FAQ:

How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 

15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals.

Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc.

Advantages? Superior quality, affordable price, professional services and technical support, fast delivery.

Quality AssuranceStrict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.

SamplesMost products provide free samples for quality evaluation, shipping cost should be paid by customers.

Factory AuditFactory audit welcome. Please make an appointment in advance.

MOQ? No MOQ. Small order is acceptable.

Delivery Time? If within stock, three days delivery guaranteed.

TransportationBy Express (FedEx, DHL), by Air, by Sea.

Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided.

Custom SynthesisCan provide custom synthesis services to best fit your research needs.

Payment TermsProforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc. 

110-52-1 - Risk and Safety:

Risk Codes
R25 - Toxic if swallowed
R37/38 - Irritating to respiratory system and skin.
R41 - Risk of serious damage to eyes
R36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description
S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S39 - Wear eye / face protection.
S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S37/39 - Wear suitable gloves and eye/face protection
UN IDs UN 2810 6.1/PG 3
WGK Germany 2
RTECS EJ7565000
TSCA Yes
Hazard Class 6.1(b)
Packing Group III

110-52-1 - Application:

1,4-Dibromobutane (CAS: 110-52-1) is used as an intermediate involved in the synthesis of active pharmaceutical ingredient and other organic compounds. Organic synthesis intermediates. 1,4-Dibromobutane is used for the manufacture of aminophylline, kebiqing, expelling Qingjing, etc. 1,4-Dibromobutane is used as a catalyst in the polymerization of 2-oxazolines. Also used in the synthesis of cholinesterase inhibitors used against Alzheimer’s disease.  

110-52-1 - Production Method:

1. 1,4-Dibromobutane is derived from tetrahydrofuran by ring opening and bromination. Hydrobromic acid was added to the reaction Pan, tetrahydrofuran was added dropwise under stirring, and sulfuric acid was added dropwise, and the temperature was controlled to be below 50℃. After completion of the reaction, the mixture was stirred for 1H. The lower solution was separated by cooling, washed with soda ash solution until neutral, dried with anhydrous calcium chloride, and filtered to obtain the finished product. 

2. Derived from the bromination of 1,4-Butanediol. Hydrobromic acid was added to the reaction pot, cooled to 10℃ with stirring, and sulfuric acid was added dropwise. After completion of the addition, 1,4-Butanediol was further added dropwise at a temperature not exceeding 15℃, and the mixture was stirred for half an hour.  Incubation was performed for 6h at 100-110℃. Cool to room temperature, separate the lower liquid, wash with soda ash solution to neutral. After Dehydration of calcium chloride, 1,4-Dibromobutane was obtained by filtration.

110-52-1 - Storage and Transportation:

Store in a cool and ventilated warehouse, away from the fire. Keep the container sealed and stored away from the oxidant. Emergency handling equipment and appropriate containment materials should be provided.

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