OEM Manufacturer H-Val-OMe·HCl - 3-Iodo-4-Methylbenzoic Acid CAS 82998-57-0 Assay ≥98.0% – Ruifu

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OEM Manufacturer H-Val-OMe·HCl - 3-Iodo-4-Methylbenzoic Acid CAS 82998-57-0 Assay ≥98.0% – Ruifu Detail:

Manufacturer Supply, High Purity, Commercial Production
Chemical Name: 3-Iodo-4-Methylbenzoic Acid
CAS: 82998-57-0

Chemical Name	3-Iodo-4-Methylbenzoic Acid
Synonyms	3-Iodo-p-toluic Acid
CAS Number	82998-57-0
CAT Number	RF-PI427
Stock Status	In Stock, Production Scale Up to Tons
Molecular Formula	C8H7IO2
Molecular Weight	262.04
Melting Point	207.0 to 212.0℃
Solubility	Soluble in Methanol
Brand	Ruifu Chemical

Item	Specifications
Appearance	Off-White Crystalline Powder
Assay	≥98.0%
Loss on Drying	≤1.0%
Residue on Ignition	≤0.50%
Total Impurities	≤2.0%
Test Standard	Enterprise Standard
Usage	Pharmaceutical Intermediates

Package: Bottle, Aluminium foil bag, 25kg/Cardboard Drum, or according to customer’s requirement.

Storage Condition: Store in sealed containers at cool and dry place; Protect from light and moisture.

3-Iodo-4-Methylbenzoic Acid (CAS 82998-57-0) is used as intermediates in medicine and organic synthesis. 3-Iodo-4-Methylbenzoic Acid, Methyl-3-Iodo-4-methylbenzoate (3 g, 109 mmol, 1 eq) dissolved in MeOH (30 ml) was added sodium hydroxide (1.3 g, 327 mmol, 3 eq) followed by the addition of water (15 ml). The above solution was stirred at room temperature for 14 h. The solution was concentrated under vacuum, and then added water. The pH of the reaction was bought to 3 using Cone. HCl. The solid obtained was filtered and dried under vacuum, Yield: 2.7 g (96 percent). 1HNMR (400MHz, DMSO -d6): δ 2.44 (s, 3H), 7.45 (d, 7- 8.00 Hz ,1H), 7.85 (d, J= 3.18 Hz, IH), 8.31 (s, IH).

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